Skip to main content

Equipment - Logue Lab

Dedicated Equipment

  • Agilent GCMS system with Gerstel Multiple Sampling System (MPS). Agilent 5975C mass spectrometer and 7890 gas chromatograph. MPS sampler configured for thermal desorption, headspace, twister and liquid sampling.
The referenced media source is missing and needs to be re-embedded.

 

  • Agilent GCMS system with autosampler. Agilent 5975 inert source mass spectrometric detector with Agilent 6890 gas chromatograph.
The referenced media source is missing and needs to be re-embedded.
  • Agilent 1200 HPLC system with (left stack from bottom to top) quaternary pump, membrane degasser, solvent tray, (right stack bottom to top) chiller, autosampler, multi-wavelength UV detector and fluorometer.
The referenced media source is missing and needs to be re-embedded.
  • Agilent 1100 HPLC system with (from bottom to top) fluorescence detector, multi-wavelength UV-Vis detector, autosampler, quaternary pump, membrane degasser and solvent tray.
DSCN1952
  • Metrohm IC system with (from left to right and top to bottom) autosampler, column compartment, conductivity detector, interface, pump, pump, suppressor module.
The referenced media source is missing and needs to be re-embedded.
  • Horiba Scientific Fluoromax-4 Spectrofluorometer
The referenced media source is missing and needs to be re-embedded.
  • Raman Systems R3000-QE portable Raman spectrometer with fiber optic probe.
  • Gamry Reference-600 Potentiostat for electrochemical analysis.
  • Labconco centrifugal evaporation system with cold trap (right module).
  • Jasco UV-Vis Spectrophotometer.
  • Glove Box (6 ft).
  • Labconco Waterpro PS analytical grade water purification system.
  • Fisher brand -40oC upright freezer.
  • Revco brand -80oC upright freezer.
  • Large refrigerator/freezer unit.
  • Solid-Phase Microextraction (SPME) apparatus.
  • Solid Phase Extraction vacuum manifold.
  • AND brand analytical balance.
  • Fiber optic illuminator for DSSCs.
  • Variety of multimeters (i.e., handheld and desktop).
  • Variety of sample preparation equipment: shakers/vortexers, block heaters, microcentrifuge, pH meter, nitrogen evaporators, pipets, sonicators, rotary evaporators, homogenizer and hot plates.
  • Large glassware oven.

Departmental Equipment (available after initial training):

  • AB SCIEX 5500 Q-trap LCMSMS system with a Shimadzu Prominence UHPLC system.
  • AB SCIEX Q-star (Q-TOF) mass spectrometer.
  • Thermo LTQ.
  • Kratos high-resolution mass spectrometer with GC, HPLC, pyrolysis, FAB and continuous-flow FAB sample introduction capabilities and EI, CI or FAB sample ionization capabilities, positive- or negative-ion detection capabilities and an ESI-FTMS and MALDI-TOF mass spectrometers
  • Varian Saturn GC/MS system with EI and CI capabilities.
  • A spectroscopy lab with near-, mid- and far-IR capabilities including DRIFT and CIR sample presentation capabilities, fluorescence and time-resolved fluorescence spectrometers and scanning and diode-array UV-Vis spectrophotometers.
  • Two solid-sate NMR spectrometers: a 200 MHz spectrometer and a 400 MHz spectrometer with variable-temperature probe.
  • 200 MHz and 400 MHz high-resolution solution NMRs.

Accessible Equipment (from collaborations):

  • Scanning Electron Microscope (Hitachi S3400N-II). Can image at high vacuum and sub-atmospheric pressure; can image features of 3 nm under ideal conditions; EDX attachment that can take elemental profiles of SEM images.
  • Atomic Force Microscopes (Park Scientific AutoProbe CP and an Agilent System). Can image features of 1 nm and is capable of imaging solid samples in contact, non-contact and intermittent contact modes).
  • Automated Dionex Accelerated Solvent Extraction systems (2) and a Supercritical Fluid Extraction system.
  • Rainin gradient HPLC systems (2) with radiochemical, refractive index, fluorescence and UV-Vis detectors.
  • Size-exclusion chromatograph with an evaporative light scattering detector.
  • Micro/nanoelectronics fabrication facility.
  • Agilent UV-Vis spectrophotometer.
  • Thermo Nicholet IR system.
  • Micromeritics ASAP 2000 surface area analyzer.

Facilities

  • Three laboratories (480 square feet each).
  • Nine dedicated laboratory computers.
  • Eight fume hoods.